|
|
Corrosion protection of ZE10 and ZE41 magnesium alloys with fluoride conversion coatings
Matějka, Lukáš ; Tkacz, Jakub (referee) ; Fintová, Stanislava (advisor)
The diploma thesis deals with preparation of fluoride conversion coatings and evaluation of electrochemical corrosion characteristics of magnesium alloys ZE10 and ZE41 in SBF solution. The main aim of the work is to increase the corrosion resistance of the investigated magnesium alloys using fluoride conversion coatings. The influence of the conditions of the preparation of the conversion coatings on their morphology and the corrosion resistance of the coated alloys will be studied. The electrochemical corrosion characteristics of the magnesium alloys with conversion coatings will be evaluated by potentiodynamic and electrochemical impedance spectroscopy.
|
|
|
Preparation and evaluation of fluoride conversion coating created on AZ31 wrought magnesium alloy
Matějka, Lukáš ; Wasserbauer, Jaromír (referee) ; Fintová, Stanislava (advisor)
The aim of this work is optimization of preparation parameters of fluoride conversion coating on the wrought magnesium alloy AZ31 in Na[BF4] melt. The monitored factors for determining quality of the prepared coatings are homogeneity of the coating surface on ground and polished samples of magnesium alloy, mechanical properties of the coating (adhesion and hardness) and the coating thickness. The main parameter was the change in these properties at different exposition times of the material to the salt melt. Coating surfaces were documented on an inverted light microscope with the addition of images representative samples using SEM. The coating thickness was documented with inverted light microscope using a polarization filter. The chemical composition was determined on three representative samples using an energy-dispersive X-ray spectrometer. The mechanical properties of the coatings were determined by scratch test on REVETEST Scratch Testing System with detector of acoustic emissions. The resulting scratches were documented on a light microscope. It was proved that polished samples exhibit superior coating in respect with ground samples, wherein the coating did not fill the trench after the finish treatment (grinding). Constant chemical composition has been demonstrated in all the coatings. Polished sample after 2 hours of exposure in the Na [BF 4] melt exhibits best mechanical properties. The obtained data are of practical importance in the use of the alloy AZ31 in various fields of industry, medicine and other research.
|
|
|
Corrosion protection of ZE10 and ZE41 magnesium alloys with fluoride conversion coatings
Matějka, Lukáš ; Tkacz, Jakub (referee) ; Fintová, Stanislava (advisor)
The diploma thesis deals with preparation of fluoride conversion coatings and evaluation of electrochemical corrosion characteristics of magnesium alloys ZE10 and ZE41 in SBF solution. The main aim of the work is to increase the corrosion resistance of the investigated magnesium alloys using fluoride conversion coatings. The influence of the conditions of the preparation of the conversion coatings on their morphology and the corrosion resistance of the coated alloys will be studied. The electrochemical corrosion characteristics of the magnesium alloys with conversion coatings will be evaluated by potentiodynamic and electrochemical impedance spectroscopy.
|
|
|
Preparation and evaluation of fluoride conversion coating created on AZ31 wrought magnesium alloy
Matějka, Lukáš ; Wasserbauer, Jaromír (referee) ; Fintová, Stanislava (advisor)
The aim of this work is optimization of preparation parameters of fluoride conversion coating on the wrought magnesium alloy AZ31 in Na[BF4] melt. The monitored factors for determining quality of the prepared coatings are homogeneity of the coating surface on ground and polished samples of magnesium alloy, mechanical properties of the coating (adhesion and hardness) and the coating thickness. The main parameter was the change in these properties at different exposition times of the material to the salt melt. Coating surfaces were documented on an inverted light microscope with the addition of images representative samples using SEM. The coating thickness was documented with inverted light microscope using a polarization filter. The chemical composition was determined on three representative samples using an energy-dispersive X-ray spectrometer. The mechanical properties of the coatings were determined by scratch test on REVETEST Scratch Testing System with detector of acoustic emissions. The resulting scratches were documented on a light microscope. It was proved that polished samples exhibit superior coating in respect with ground samples, wherein the coating did not fill the trench after the finish treatment (grinding). Constant chemical composition has been demonstrated in all the coatings. Polished sample after 2 hours of exposure in the Na [BF 4] melt exhibits best mechanical properties. The obtained data are of practical importance in the use of the alloy AZ31 in various fields of industry, medicine and other research.
|
guest ::
